Optimization of Essential Oils Microwave Assisted Extraction Process of Peperomia subspathulata in Colombian Southwest

dc.creatorPérez-Pazos, Valeria
dc.creatorArturo-Perdomo, David
dc.creatorMujica-Martínez, Cesar A.
dc.creatorMaldonado-Rodríguez, Jhon Ironzi
dc.creatorVargas-Gallego, Juan Camilo
dc.date2025-10-08
dc.descriptionEssential oil extraction is an area of study that is advancing with the implementation of new extraction methods in the search for new chemotypes, improved yields, and reduced energy consumption. It is applied in the agroindustry and pharmaceutical sciences, among others. In this study, new technologies for extracting volatiles from Colombian plant species were explored, focusing on parameter optimization through an experimental design using microwave radiation. The objective was to optimize power and time parameters to maximize the yield of essential oils of Peperomia subspathulata, a species that had not been studied before in the Nariño department. The methodology consisted of microwave-assisted hydrodistillation under a 32-factorial design and the response surface method. The chemical profile was obtained through gas chromatography and mass spectrometry, and the yields were compared. The results obtained in this study were as follows: the optimal microwave parameters were 800 W and 81 minutes, with a yield of 1.49% for leaves and 0.99% for stems, values higher than those of conventional hydrodistillation (1.15% and 0.84%, respectively). The chemical profile of the essential oils revealed a new chemotype composed of Myristicin, Safrole, and alpha-bisabolol in both methods. Likewise, the chromatographic areas of these components were optimized, obtaining values of 46.88% for Safrole, 58.84% for Myristicin and 18.58% for alpha-bisabolol. In conclusion, this study establishes the implementation of an innovative extraction methodology with high yields and reduced times; moreover, a new chemotype for P. subspathulata from the Nariño province, laying the foundation for the study of other aromatic species in future research.en-US
dc.descriptionLa extracción de aceites esenciales es un área de estudio que avanza con la implementación de nuevos métodos de extracción en la búsqueda de nuevos quimiotipos, mejores rendimientos y reducción del consumo energético, siendo aplicada en campos como la agroindustria, las ciencias farmacéuticas, entre otras. En este estudio se exploraron nuevas tecnologías para la extracción de volátiles en especies vegetales colombianas, enfocándose en la optimización de parámetros a través de un diseño experimental, utilizando radiación de microondas. El objetivo fue optimizar los parámetros de potencia y tiempo para maximizar el rendimiento de aceites esenciales de Peperomia subspathulata, una especie sin estudios previos en el departamento de Nariño. La metodología empleada consistió en el uso de la hidrodestilación asistida por microondas bajo un diseño factorial 32 y el método de superficie de respuesta para obtener el perfil químico a través de cromatografía de gases y espectrometría de masas, y comparar los rendimientos. Los resultados obtenidos en este estudio fueron los siguientes: los parámetros óptimos por microondas fueron 800 W y 81 minutos, obteniendo un rendimiento de 1,49 % para hojas y 0,99 % para tallos, valores superiores a los de la hidrodestilación convencional (1,15 % y 0,84 %, respectivamente). El perfil químico de los aceites esenciales reveló un nuevo quimiotipo compuesto por Miristicina, Safrol y alfa-bisabolol en ambos métodos. Asimismo, se optimizaron las áreas cromatográficas de estos componentes, obteniendo valores de 46,88 % para Safrol, 58,84 % para Miristicina y 18,58 % para alfa-bisabolol. En conclusión, esta investigación implementa una metodología innovadora de extracción con altos rendimientos y tiempos reducidos, además un nuevo quimiotipo para P. subspathulata del departamento de Nariño sentando las bases para el estudio de otras especies aromáticas en futuras investigaciones.es-ES
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dc.identifierhttps://revistas.itm.edu.co/index.php/tecnologicas/article/view/3371
dc.identifier10.22430/22565337.3371
dc.languagespa
dc.publisherInstituto Tecnológico Metropolitano (ITM)en-US
dc.relationhttps://revistas.itm.edu.co/index.php/tecnologicas/article/view/3371/3798
dc.relationhttps://revistas.itm.edu.co/index.php/tecnologicas/article/view/3371/3905
dc.relationhttps://revistas.itm.edu.co/index.php/tecnologicas/article/view/3371/3907
dc.relationhttps://revistas.itm.edu.co/index.php/tecnologicas/article/view/3371/4019
dc.relationhttps://revistas.itm.edu.co/index.php/tecnologicas/article/view/3371/4096
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dc.relation/*ref*/E. Ramazani, M. Akaberi, S. Ahmad Emami, and Z. Tayarani-Najaran, “Pharmacological and biological effects of alpha-bisabolol: An updated review of the molecular mechanisms,” Life Sci., vol. 304, p. 120728, Sep. 2022. https://doi.org/10.1016/j.lfs.2022.120728
dc.relation/*ref*/R. L. Smith et al., “GRAS Flavoring Substances 24 The 24th publication by the FEMA expert Panel presents safety and usage data on 236 new generally recognized as safe flavoring ingredients,” Food Technol., vol. 63, no. 6, pp. 46-105, 2009. https://www.femaflavor.org/publications/gras-publications/gras-24
dc.relation/*ref*/L. J. Marnett et al., “GRASr2 Evaluation of Aliphatic Acyclic and Alicyclic Terpenoid Tertiary Alcohols and Structurally Related Substances Used as Flavoring Ingredients,” J. Food Sci., vol. 79, no. 4, pp. 428-441, Apr. 2014. https://doi.org/10.1111/1750-3841.12407
dc.relation/*ref*/
dc.rightsCopyright (c) 2025 TecnoLógicasen-US
dc.rightshttps://creativecommons.org/licenses/by-nc-sa/4.0en-US
dc.sourceTecnoLógicas; Vol. 28 No. 64 (2025); e3371en-US
dc.sourceTecnoLógicas; Vol. 28 Núm. 64 (2025); e3371es-ES
dc.source2256-5337
dc.source0123-7799
dc.subjectcongonaes-ES
dc.subjectdiseño experimentales-ES
dc.subjecthidrodestilación clevengeres-ES
dc.subjectquimiotipoes-ES
dc.subjectPiperaceases-ES
dc.subjectcongonaen-US
dc.subjectdesign methodologyen-US
dc.subjectclevenger hydrodistillationen-US
dc.subjectchemotypeen-US
dc.subjectPiperaceaeen-US
dc.titleOptimization of Essential Oils Microwave Assisted Extraction Process of Peperomia subspathulata in Colombian Southwesten-US
dc.titleOptimización del proceso de extracción asistido por microondas de aceites esenciales de Peperomia subspathulata en el suroccidente colombianoes-ES
dc.typeinfo:eu-repo/semantics/article
dc.typeinfo:eu-repo/semantics/publishedVersion
dc.typeResearch Papersen-US
dc.typeArtículos de investigaciónes-ES

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